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This invention relates to the nitration of organic compounds, particularly aromatic compounds, and more particularly to the improvement of the reaction carried out in a reactor which is internally packed with a solid.
2. Description of the Prior Art
Nitration is a multi-billion dollar chemical industry. In nitration, compounds of certain types are reacted with nitric acid in the presence of sulfuric acid to form nitrated derivatives which are useful in synthetic organic chemistry. In one such process aryl carboxylic acids, such as benzoyl alcohol, are nitrated by nitration with molecular oxygen. Typically, the reaction mixture is conducted in the presence of sulfuric acid, nitric acid, and an inert diluent, such as an aqueous solution of the acid. The nitric acid oxidizes the carboxyl group in the carboxylic acid to form a nitric oxide group, nitrate, and the aqueous sulfuric acid dissolves the carbonate group to form a sulfonic acid.
When nitration of an organic compound is done in a liquid phase, the solvent can be employed in the reaction both as a diluent for the acid and for the nitrate. The diluent is employed, however, only to serve as a convenient means for transferring the reaction mixture from one vessel to another.
The prior art, therefore, has proposed a number of apparatus for carrying out the nitration reaction, in which a reactive mixture is passed through a filter of stainless steel or like material, as the name suggests, or a similar material which can be used as a filter. The efficiency of such a filter may be improved by the incorporation of a highly porous, relatively permeable material within the filter. Some of the prior art apparatus employs a packed material such as sand or like material to hold the reactive mixture.
One method of contacting an organic material with a solid in a reactor vessel is disclosed in U.S. Pat
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